TY  - JOUR
A1  - Saeed, Aamer
A1  - Shaheen, Uzma
A1  - Bolte, Michael
T1  - Synthesis and Crystal Structure of 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea
T2  - Crystals
N2  - The title thiourea was synthesized by reaction of 3,4,5-trimethoxybenzoyl isothiocyante with 3-fluoroaniline. The 3,4,5-trimethoxybenzoyl isothiocyante was produced in situ by reaction of 3,4,5-trimethoxybenzoyl chloride with ammonium thiocyanate in dry acetonitrile. The structure was confirmed by the spectroscopic, elemental analysis and single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21/c with unit cell dimensions a = 13.0966(9), b = 16.6460(13), c = 7.8448(5), β = 106.721(5)°, V 1637.9(2) ų, Z = 4.
KW  - Synthesis
KW  - 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea
KW  - crystal structure
Y1  - 2011
UR  - http://publikationen.ub.uni-frankfurt.de/frontdoor/index/index/docId/25268
UR  - https://nbn-resolving.org/urn:nbn:de:hebis:30:3-252688
SN  - 2073-4352
VL  - 1.2011
IS  - 2
SP  - 34
EP  - 39
PB  - Molecular Diversity Preservation International (MDPI)
CY  - Basel
ER  -