TY - JOUR A1 - Ruth, Kai A1 - Morawitz, Thorsten A1 - Lerner, Hans-Wolfram A1 - Bolte, Michael T1 - [my]-Hydroxido-bis[(2,20-bipyridine)-tricarbonylrhenium(I)] perrhenate T2 - Acta crystallographica / Section E, Structure reports online N2 - The title compound, [Re2(OH)(C10H8N2)2(CO)6][ReO4], is a mixed-valence rhenium compound containing discrete anions and cations. The ReI atoms are in a slightly distorted octahedral environment, whereas the ReVII atoms show the typical tetrahedral coordination mode. The dihedral angle between the two bipyridine groups is 34.3 (7)°. Key indicators: single-crystal X-ray study; T = 173 K; mean σ(C–C) = 0.044 Å; R factor = 0.093; wR factor = 0.262; data-to-parameter ratio = 13.9. Y1 - 2008 UR - http://publikationen.ub.uni-frankfurt.de/frontdoor/index/index/docId/6980 UR - https://nbn-resolving.org/urn:nbn:de:hebis:30-69773 N1 - This is an open-access article distributed under the terms of the Creative Commons Attribution Licence http://creativecommons.org/licenses/by/2.0/uk/legalcode, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. VL - 64 IS - m496 ER -