Die Kristallstruktur der Verbindung N-Trimethylsilyl-3,4-Dimethylpyridiniumbromid
The crystal structure of N-trimethylsilyl-3,4-dimethylpyridinium bromide
- Trimethylbromosilane and 3,4-lutidine form a 1:1 compound which is stable at room temperature. Single crystals of this compound can be isolated by sublimation. It crystallizes in the orthorhombic space group P 2121,21, with lattice constants a = 737,08(9) pm, b = 1295,7(1) pm, c = 1318,8(3) pm. The crystal structure was refined to Rw = 0,042 and proves an ionic structure.
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| Author: | Karl Hensen, Peter Wagner |
|---|---|
| URN: | urn:nbn:de:hebis:30:3-816819 |
| DOI: | https://doi.org/10.1515/znb-1993-0117 |
| ISSN: | 1865-7117 |
| ISSN: | 0932-0776 |
| Parent Title (German): | Zeitschrift für Naturforschung, B |
| Publisher: | Verlag der Zeitschrift für Naturforschung |
| Place of publication: | Tübingen |
| Document Type: | Article |
| Language: | German |
| Date of Publication (online): | 2014/06/02 |
| Year of first Publication: | 1993 |
| Publishing Institution: | Universitätsbibliothek Johann Christian Senckenberg |
| Release Date: | 2024/01/18 |
| Tag: | 3,4-Dimethylpyridine; Addition Compound; Crystal Structure; Trimethylbromosilane |
| Volume: | 48.1993 |
| Issue: | 1 |
| Page Number: | 3 |
| First Page: | 79 |
| Last Page: | 81 |
| Note: | Vorabveröffentlichung von Teilen der Dissertation von Peter Wagner: Untersuchungen von Schmelzdiagrammen binärer Systeme bestehend aus Trimethylbromsilan und den isomeren Lutidinen. Frankfurt (Main), Univ., Diss., 1992 |
| Institutes: | Biochemie, Chemie und Pharmazie / Biochemie und Chemie |
| Dewey Decimal Classification: | 5 Naturwissenschaften und Mathematik / 54 Chemie / 540 Chemie und zugeordnete Wissenschaften |
| Sammlungen: | Universitätspublikationen |
| Licence (German): |  Creative Commons - Namensnennung-Nicht kommerziell-Keine Bearbeitung 3.0 |
