(1R,2S)-Methyl 1-(4-chloro-phen-yl)-3-oxo-1,2,3,4-tetra-hydro-cyclo-penta-[b]indole-2-carboxyl-ate 0.2-hydrate
- The title compound, C(19)H(14)ClNO(3)·0.2H(2)O, crystallizes with five mol-ecules and a disordered water mol-ecule in the asymmetric unit. Four of the five mol-ecules form hydrogen-bonded dimers via N-H⋯O hydrogen bonds towards another symmetry-independent mol-ecule, whereas the fifth mol-ecule forms a hydrogen-bonded dimer with its symmetry equivalent, also via N-H⋯O hydrogen bonds. The dihedral angle between the planes of the fused benzene ring and the five-membered ring to which it is attached is 79.45 (13), 49.00 (15), 72.49 (16), 81.91 (18) and 76.38 (16)° for the five mol-ecules in the asymmetric unit.
Author: | Sadiya Raja, Michael BolteORCiD |
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URN: | urn:nbn:de:hebis:30:3-252718 |
DOI: | https://doi.org/10.1107/S1600536811042358 |
ISSN: | 1600-5368 |
Pubmed Id: | https://pubmed.ncbi.nlm.nih.gov/22220011 |
Parent Title (English): | Acta crystallographica / Section E, Structure reports online |
Publisher: | Munksgaard |
Place of publication: | Copenhagen |
Document Type: | Article |
Language: | English |
Date of Publication (online): | 2011/10/22 |
Date of first Publication: | 2011/10/22 |
Publishing Institution: | Universitätsbibliothek Johann Christian Senckenberg |
Release Date: | 2012/06/25 |
Volume: | 67 |
Issue: | o2991 |
Page Number: | 22 |
HeBIS-PPN: | 35757463X |
Institutes: | Biochemie, Chemie und Pharmazie / Biochemie und Chemie |
Dewey Decimal Classification: | 5 Naturwissenschaften und Mathematik / 54 Chemie / 540 Chemie und zugeordnete Wissenschaften |
Sammlungen: | Universitätspublikationen |
Licence (German): | Creative Commons - Namensnennung 3.0 |