TY - JOUR A1 - Fenske, Dieter A1 - Hollnagel, Achim A1 - Merzweiler, Kurt T1 - Zur Reaktion von [(η3-C4H7)PdCl]2 mit Se(SiMe3)2. Die Kristallstruktur von [(η3-C4H7)6Pd6Se3] T1 - Reaction of [(η3-C4H7)PdCl]2 with Se(SiMe3)2. The crystal structure of [(η3-C4H7)6Pd6Se3] T2 - Zeitschrift für Naturforschung, B N2 - [(η3-C4H7)PdCl]2 reacts with Se(SiMe3)2 to form [(η3-C4H7)6Pd6Se3] (1). 1 has been characterized by X-ray crystal structure analysis. It contains a distorted trigonal prismatic Pd6-cluster. Three faces of the Pd-prism are occupied by μ4-Se ligands. 1 crystallizes in the space group Pnma with 4 formula units per unit cell. The lattice constants at 200 K are: a = 1175.1(8), b = 1611.4(12), c = 1720.3(12) pm. KW - Synthesis KW - X-Ray KW - Crystal Structure of [(η3-C4H7)6Pd6Se3] KW - Trigonal Prismatic Pd-Se Cluster Y1 - 2014 UR - http://publikationen.ub.uni-frankfurt.de/frontdoor/index/index/docId/72188 UR - https://nbn-resolving.org/urn:nbn:de:hebis:30:3-721882 SN - 1865-7117 SN - 0932-0776 VL - 43.1988 IS - 5 SP - 634 EP - 636 PB - Verlag der Zeitschrift für Naturforschung CY - Tübingen ER -