TY - JOUR A1 - Hensen, Karl A1 - Wagner, Peter T1 - Die Kristallstruktur der Verbindung N-Trimethylsilyl-3,4-Dimethylpyridiniumbromid T1 - The crystal structure of N-trimethylsilyl-3,4-dimethylpyridinium bromide T2 - Zeitschrift für Naturforschung, B N2 - Trimethylbromosilane and 3,4-lutidine form a 1:1 compound which is stable at room temperature. Single crystals of this compound can be isolated by sublimation. It crystallizes in the orthorhombic space group P 2121,21, with lattice constants a = 737,08(9) pm, b = 1295,7(1) pm, c = 1318,8(3) pm. The crystal structure was refined to Rw = 0,042 and proves an ionic structure. KW - Trimethylbromosilane KW - 3,4-Dimethylpyridine KW - Addition Compound KW - Crystal Structure Y1 - 2014 UR - http://publikationen.ub.uni-frankfurt.de/frontdoor/index/index/docId/81681 UR - https://nbn-resolving.org/urn:nbn:de:hebis:30:3-816819 SN - 1865-7117 SN - 0932-0776 N1 - Vorabveröffentlichung von Teilen der Dissertation von Peter Wagner: Untersuchungen von Schmelzdiagrammen binärer Systeme bestehend aus Trimethylbromsilan und den isomeren Lutidinen. Frankfurt (Main), Univ., Diss., 1992 VL - 48.1993 IS - 1 SP - 79 EP - 81 PB - Verlag der Zeitschrift für Naturforschung CY - Tübingen ER -