TY - JOUR A1 - Kresze, Günter A1 - Lodemann, Edgar A1 - Wacker, Adolf T1 - Über die O-Trifluoracetylierung von Nucleosiden T2 - Zeitschrift für Naturforschung, B N2 - The trifluoroacetylation of thymidine at room temperature was performed using trifluoroacetic acid phenylester in pyridine. A selective protection of the 5′-position was not possible: Even low molar quantities of the trifluoroacetylating agent gave rise to bis-trifluoroacetylation. The bis-trifluoroacetyl derivatives of thymidine and 5-bromo-deoxyuridine were purified by vacuum sublimation. The completely trifluoroacetylated deoxyribosides of uracil, 5-iodouracil and adenine underwent decomposition during sublimation. Y1 - 2014 UR - http://publikationen.ub.uni-frankfurt.de/frontdoor/index/index/docId/74871 UR - https://nbn-resolving.org/urn:nbn:de:hebis:30:3-748714 SN - 1865-7117 SN - 0932-0776 N1 - Die vorliegende Arbeit ist ein Teil der Dissertation von E. LODEMANN, Technische Hochschule, München 1963. VL - 22 IS - 3 SP - 285 EP - 287 PB - Verlag der Zeitschrift für Naturforschung CY - Tübingen ER -