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- 2008 (1)
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- Englisch (1)
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Schlagworte
- Fmoc solid phase peptide synthesis (1) (entfernen)
Institut
- Zentrum für Biomolekulare Magnetische Resonanz (BMRZ) (1) (entfernen)
A mild synthetic method for N-formyl-Met-Leu-Phe-OH (1) is described. After Fmoc solid phase peptide synthesis, on-bead formylation and HPLC purification, more than 30 mg of the fully 13C/15N-labelled tripeptide 1 could be isolated in a typical batch. This peptide can be easily crystallised and is therefore well suited as a standard sample for setting up solid-state NMR experiments.