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By analyzing the phase diagrams of some trimethylhalogenosilane/pyridine- and methyl-trichlorosilane/lutidine-systems the existence of the incongruently melting addition compounds Me3SiF · (Pyridine)2, Me3SiCl · (Pyridine)2, MeSiCl3, · (2.5-Lutidine)2, MeSiCl3, · (2.6-Lutidine)2, (MeSiCl3)2 · 3.5-Lutidine, and the congruently melting compounds MeSiCl3 · 2.4-Lutidine, MeSiCl3 · (3.5-Lutidine)2 was proven.
A new evaluation of DSC-curves of binary mixtures is given. By analyzing the phase diagrams of methyltrichlorosilane and dimethyldichlorosilane with some lutidines the existence of the incongruently melting addition compounds MeSiCl3 · (2.3-Lutidine)-,, MeSiCl3 · 2.3-Lutidine, (MeSiCl3)2 · 3.4-Lutidine, Me,SiCl2 · (2.3-Lutidine)2, Me2SiCl2 · (2.5-Lutidine),, Me2SiCl2 · 2.5-Lutidine, Me2SiCl2 · (2.6-Lutidine)2, Me2SiCl2 · 2.6-Lutidine, Me2SiCl2 · (3.4-Lutidine)2, Me,SiCl2 · 3.4-Lutidine, (Me2SiCl2)2 · 3.4-Lutidine, Me2SiCl2 · (3.5-Lutidine)2, Me2SiCl2 · 3.5-Lutidine, and the congruently melting compound MeSiCl3 ·(3.4-Lutidine)2 was proven.