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Biacetylbis(methylimine) (1) is obtained by formic acid catalyzed condensation of biacetyl and methylamine. Photoelectron- and UV spectra, H NMR and 13C NMR data are compared with those of the new compound biacetylbis(isopropylimine) (2) and glyoxalbis(isopropylimine) (3).