Synthesis and Crystal Structure of 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea
- The title thiourea was synthesized by reaction of 3,4,5-trimethoxybenzoyl isothiocyante with 3-fluoroaniline. The 3,4,5-trimethoxybenzoyl isothiocyante was produced in situ by reaction of 3,4,5-trimethoxybenzoyl chloride with ammonium thiocyanate in dry acetonitrile. The structure was confirmed by the spectroscopic, elemental analysis and single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21/c with unit cell dimensions a = 13.0966(9), b = 16.6460(13), c = 7.8448(5), β = 106.721(5)°, V 1637.9(2) ų, Z = 4.
Author: | Aamer SaeedORCiD, Uzma Shaheen, Michael BolteORCiD |
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URN: | urn:nbn:de:hebis:30:3-252688 |
DOI: | https://doi.org/10.3390/cryst1020034 |
ISSN: | 2073-4352 |
Parent Title (English): | Crystals |
Publisher: | Molecular Diversity Preservation International (MDPI) |
Place of publication: | Basel |
Document Type: | Article |
Language: | English |
Date of Publication (online): | 2012/06/27 |
Date of first Publication: | 2011/05/09 |
Publishing Institution: | Universitätsbibliothek Johann Christian Senckenberg |
Release Date: | 2012/06/27 |
Tag: | 1-(3-fluorophenyl)-3-(3,4,5-trimethoxybenzoyl)thiourea; Synthesis; crystal structure |
Volume: | 1.2011 |
Issue: | 2 |
Page Number: | 6 |
First Page: | 34 |
Last Page: | 39 |
HeBIS-PPN: | 357574052 |
Institutes: | Biochemie, Chemie und Pharmazie / Biochemie und Chemie |
Dewey Decimal Classification: | 5 Naturwissenschaften und Mathematik / 54 Chemie / 540 Chemie und zugeordnete Wissenschaften |
Sammlungen: | Universitätspublikationen |
Licence (German): | Creative Commons - Namensnennung 3.0 |